Exodus 9:1
Then the Lord said unto Moses, Go in unto Pharaoh, and tell him, Thus saith the Lord God of the Hebrews, Let my people go, that they may serve me.
Cross-reference
Exodus 3:18 first records the command to request a three-day journey—now repeated as the consistent divine demand to let Israel serve God.
Exodus 4:22 introduces the same 'Thus says the LORD' formula and identifies Israel as God's firstborn—the basis for the demand.
Exodus 4:23 contains the identical demand 'Let my son go that he may serve me'—here applied to the whole people.
Exodus 5:1 is the first fulfillment of this command when Moses and Aaron actually deliver it to Pharaoh.
Exodus 8:1 has the exact same command for the plague of frogs—showing this pattern repeated for each plague.
Exodus 8:20 repeats this command for the plague of flies, with the added detail of meeting Pharaoh at the water.
Exodus 10:3 includes a rebuke 'How long will you refuse to humble yourself?' before the same demand—highlighting Pharaoh's hardness.
Exodus 7:16 is the first occurrence of this demand, for the plague of blood—the initial warning to Pharaoh.